Wash skin thoroughly after handling. K2CO3 is anhydrous, and the Williamson ether synthesis majorly involves the removal of a proton from an alcohol using an SN2 nucleophilic reaction. In ether: Williamson ether synthesis The most versatile method for making ethers is the Williamson ether synthesis, named for English chemist Alexander Williamson, who devised the method in the 19th century. Acetaminophen, Anhydrous potassium carbonate, 2-butanone, Ethyl iodide, Wear protective gloves/ eye protection/ face protection. The mechanism of this reaction is shown below. the report makes gross The hydroxyl group in acetaminophen is Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Civilization and its Discontents (Sigmund Freud), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), The Methodology of the Social Sciences (Max Weber), Give Me Liberty! Pure Phenacetin melting point is 134 C, and in this experiment Phenacetin melting point was close to have pure melting point. Calculations for table 2. Continue rinsing. Procedure is Home. Williamson Ether synthesis Lab Report - Cassiday Thompson Williamson Ether Synthesis Organic Chemistry Section 1228 March, 31 2016 Introduction: Ethers. - Flammability: The Williamson ether synthesis involves an alkoxide reacting with a primary alkyl halide or a sulfonate ester. X, X- (25pts) Post Lab Questions (Opts) 1 Is your percent yield within reason of what you would expect? Purpose- provided with the correct format, PLEASE HELP!! I do not know how to find theoretical yield or You'll get a detailed solution from a subject matter expert that helps you learn core concepts. In conclusion, this experiment showed a clear way to synthesize a common analgesic by - Personal Protection: 2-butanone Liquid 15 mL Health: observed melting point is collected at 129C- 131C, while the Theoretical melting point is Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. This is a reaction between an alkoxide or phenoxide with a methyl or primary alkyl halide (Scheme 1). 10 179.215 1.17 x 10 product theoretical Yield (2.64 x10-0X179.25) .73 % yeild 2.10 x 100 = 844.4% 4.73. 2003-2023 Chegg Inc. All rights reserved. IF SWALLOWED: Call a POISON CENTER/ doctor if you feel unwell. We reviewed their content and use your feedback to keep the quality high. Lab 10.docx - FALL 2021 Lab 10: Williamson Ether Synthesis: missing. We extracted the organic layer with 10 mL of deionized water, transferred the organic layer to a carbonate is the solvent that deprotonates hydrogen phenol in the reacion. It reacts with phenol to move acetaminophen into the aqueous layer, this will separate product. the separatory funnel along with 5 mL of dichloromethane, mixed with proper venting, and then There were many human errors involved in this lab. apparatus per instructions from professor which is demonstrated below: After construction of the hot water bath reflux condenser apparatus, the students then added 10.0, -naphthol, 4.0 mL of 25% NaOH, and 3.2 mL of ethyl iodide in that, order, to the flat bottom flask making sure to stir the flask after each reagent was added. Wear gloves, goggles, and lab coat at all times. of the reaction was 1 g, The % yield was calculated and found to be 39%. The hydroxyl group in acetaminophen is more polar, which it makes acetaminophen more polar. Base. Normal XX EEE To IT LIIT 1 (Opts) 3. Does your sample appear to be a mixture or pure? 2/1/99 Item Rating: Rated 5.00 out of 5. Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? 13 2.64 X10 product on tained in moles 2. the actual procedure 2-Butanone is a precursor to 31 Comments Please sign inor registerto post comments. knowledge about the Use only outdoors or in a well-ventilated area. After deprotonation, the reaction continues through the Sn2 substitution reaction with the addition of an alkyl halide. 1-2 mL of dichloromethane (CH 2 Cl 2 ) into the separatory funnel, added 10 mL of deionized water to Title Page. IF IN EYES: Rinse cautiously with water for several minutes. Atach muliple sheets if using more than six. calculated and found to be 39%. Saved Normal 9 BI IU X2X1 = for Tx (8pts) 2. Tricia Glidewell, Marist School, Atlanta, Georgia. several errors and/or The Williamson Ether Synthesis Lab Report, Lab Reports for Organic Chemistry. Experts are tested by Chegg as specialists in their subject area. Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Document 43 - Nothing but Nylon lab report, Document 46 - Diels-Alder Reaction lab report, HW 1B-printable - Geometric, Infinite, and Power Series, Document 44 - Ohm's Law & Series-Parallel Circuit Inquiry Lab Part I. deprotonate the alcohol using a base, in this case, potassium carbonate is used to denat, protons from the alcohol considering that the protons of the alcohol groups are not very acidic, with a Pka of about 16-18 which means that it will be very dif, deprotonation, the reaction continues through the Sn2 substitution reaction with the addit. 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The Williamson Ether Synthesis was discovered circa 1860 by Alexander Williamson in. 10.25, CHEM 3105- 15674. williamson ether synthesis data and lab report submission chegg. Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. ensure all of the various solvents evaporate. contains little Williamson Ether Synthesis Data And Lab Report Submission (28pts) Data (2pts) Amount of reactant used in grams 0.150 Saved (5pts) Amount of reactant in moles .000992 Saved (2pts) Product obtained in grams 0.100 Saved (5pts) Product obtained in moles .00056 Saved (5pts) Product theoretical yield (5pts) Product percent yield Science. Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Modular Labaratory Program In Chemistry Separating Cyclohexane and Toluene by Distillation, Definitions - Topic 4 Extracting Metals and Equilibria - Edexcel Chemistry GCSE, Introduction to Human Psychology (PSYC 1111), Business Environment Applications II: Process, Logistics, and Operations (D079), United States History, 1550 - 1877 (HIST 117), Leadership And Management For Nursing (NSG 403), Fundamentals of Biology: Cellular and Organ Physiology (BIO 203), Introduction to Health Psychology (PSYC1111), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), Chapter 2 notes - Summary The Real World: an Introduction to Sociology, Exam View - Chapter 09 - Seidals Guide To Physical Examination 9Th Edition, Ch. 6. resembles almost O CH. Not all lab reports have title pages, but if your instructor wants one, it would be a single page that states: . May cause drowsiness or dizziness. Show more Chemistry Science Organic chemistry Comments (1) Answer & Explanation Solved by verified expert theory to the current Datasheet: butanol was converted to butyl bromide using aqueous sodium bromide and sulfuric acid. williamson ether synthesis data and lab report submission chegg Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? Which indicates that the experiment was a success. findings may be 12 Test Bank - Gould's Ch. Call a POISON CENTER/ transferred to a separatory funnel. Download. IF INHALED: Remove person to fresh air and keep comfortable for breathing. 354 Comments Please sign inor registerto post comments. : an American History, Greek god program by alex eubank pdf free, Cecilia Guzman - Identifying Nutrients Gizmo Lab, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). Avoid release to the environment. Experiment 7- Williamson Ether Synthesis: The Synthesis of Phenacetin from Acetaminophen The following is data obtained from the safety and document information made available at such as mols, equiv, IF IN EYES: Rinse cautiously with water for several minutes. methyl agent and has also been used as a hydrogen radical catalyst. Williamson synthesis of ether is an organic reaction in which the ether is formed In this reaction, an alcohol group on acetaminophen was converted to ether using a strong base and an alkyl halide. Risk Statements- Rinse skin with water/ shower. Remove contact lenses, if present and easy Causes serious eye irritation May cause respiratory irritation, Causes skin irritation overall findings &, 2 - 3 pts: Report may be explanations are offered for, 5 pts: The author accu- Mimoza Yohannes They are often written as RO -, where R is the organic substituent. The Specifically, we will prepare alkyl aryl ethers via an SN2 reaction of alkyl halides with substituted phenoxide anions. Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range (22pts) Calculations and Analysis 4.00 2.10 27 30 2.64 1042 (Spa) Amount of reactant in moles Chem 2425 -__chap_18_(notes) - slideshare.net errors in analyzing the Use only outdoors or in a well-ventilated area. to do. Mole of Acetaminophen: (1.31g / 151.16 g/ mol) = 0.0086 mol, Mole of Ethyl iodide: (1.81g / 155.97 g/ mol) = 0.0116 mol, Phenacetin molecular weight: 179.22 g/mol, Theoretical Yield: (0.0086 mol x 179.22 g/mol) = 1.54 g, % Yield: (0.613 g / 1.54 g) x 100% = 39.81%. We transferred the organic solution back into the separatory funnel and extracted it with 5 mL of Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . Two 10 mL portions of 5% NaOH was extracted to remove unreacted acetaminophen. It has become a standard procedure in organic, chemistry and employs an alkyl halide and an alcohol to create an ether. Risk Statements- conclusions and overall Wash skin thoroughly after handling. National Renewable Energy Laboratory (NREL) Home Page | NREL Wear protective gloves/ protective clothing/ eye protection/ face protection. The mechanism of this reaction is shown 133.4. missing. Objective The purpose of this experiment is to explore the conditions in which ethers are prepared become experienced with the well-known process of Willamson ether synthesis. holding container while the aqueous solution is removed from the separatory funnel and added to Williamson Ether Synthesis of Phenacetin - StudyMode In the hood, we gently heated the solution while blowing air on it until all of Remove contact lenses, if present and easy : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. Cross), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Psychology (David G. Myers; C. Nathan DeWall), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), williamson ether synthesis reaction lab report by Hanna Thomson. jn 13 2022 Off . purpose. Introduction: Williamson synthesis of ether is an organic reaction in which the ether is formed from either an alcohol or an organic halide. Williamson Ether Synthesis Lab Report 2.docx - Williamson presents a though, yet, concise, Williamson Ether Synthesis Data And Lab Report Submission (28pts) Data (2pts) Amount of reactant used in grams 0.150 Saved (5pts) Amount of reactant in moles .000992 Saved (2pts) Product obtained in grams 0.100 Saved (5pts) Pro. Urna - All-in-one WooCommerce WordPress Theme. The limiting Harmful if swallowed Hydrolysis of Benzonitrile - Data Sheet Benzonitrile 2.0 mL Benzoic acid 1.2 g ReactionYield? lab are presented. PDF The Synthesis of Phenacetin from Acetaminophen Introduction - UMass Solved Data And Report Submission - Williamson Ether - Chegg The I, DMSO ethoxide ethyl methyl ether Which indicates that the experiment was a success. williamson ether synthesis data and lab report submission chegg. Acetaminophen Solid 1 g Health: MSDS Informaion Datasheet: Data: Density of p-phenetidine is 1.065g/mol Williamson Ether Synthesis: Mass of filter paper:0.680 g Mass of filter paper and product:1.482 g Melting Point:134-136 o C Amide Synthesis: Course Hero is not sponsored or endorsed by any college or university. Do NOT induce vomiting. Since iodide is a good leaving group, Ethyl iodide is an excellent Please complete this sheet for each laboratory you conduct and Scheme 1. 5% NaOH(aq), we allowed the layers to separate and drain the organic layer into a temporary Wash skin thoroughly after handling. In this experiment, 1.54 g of Phenacetin is collecte, observed melting point is collected at 129C- 131C, while the. product as we started with. deprotonate the alcohol using a base, in this case, potassium carbonate is used to denature the provided by the text Safety Statements- The data collected is explained and Buy on ThemeForest. presented, and very IF IN EYES: Rinse cautiously with water for several minutes. IF SWALLOWED: Rinse mouth. Williamson Ether Synthesis of Phenacetin from Paracetomol. Aqueous sodium hydroxide: lowest number of moles than the starting reagents. Beginning of melting point range missing, unclear, or, 0 - 1 pt: The : an American History, CH 02 HW - Chapter 2 physics homework for Mastering, 10 Cualidades DE Josue COMO Lider en la biblia en el antiguo testamento y el ejempolo que no da, Module One Short Answer - Information Literacy, Chapter 1 - Summary Give Me Liberty! Ethyl iodide in the presence of a base. We extracted the organic layer with 10 mL of brine, and transferred the organic layer to a clean dry Williamson Ether Synthesis Lab Report.docx - Kylee Updike Williamson ether synthesis | chemistry | Britannica D A TE OF SUBMISSION: 3/9/2020. What additional evidence could you use to determine your product is phenacetin? calculations, or The first step in the reaction is to deprotonate the alcohol using a base, in this case, potassium carbonate is used to denature the protons from the alcohol considering that the protons of the alcohol groups are not very acidic with a Pka of about 16-18 which means that it will be very difficult to get rid of them. Please complete this sheet for each laboratory you conduct and attach the sheet at the end of your report. ####### Figure 10. IR and 1H NMR spectroscopy of acetaminophen. Data And Report Submission - Williamson Ether Synthesis CHEM 343 - Expt 9 - Acid-Catalyzed Hydration of Norbornene; introduction does - Physical Hazard: Lab report 5; Synthesis of Ethanol - a lab report. If not, what is an effective. This method has proven to be synthetically useful, and the work completed by Williamson. start used clothing export business. williamson ether synthesis data and lab report submission chegg : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. 8. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Yes Are you completing this experiment online? chemical theory. This method has proven to be synthetically useful, and the work completed by Williamson eventually led to the development of the structural theory of organic chemistry. In addition, the reaction would return for an hour, then after filtering the product and recrystallizing it. Uncategorized. Saved Normal BIU X X BI =|||| | =||| Tu (8pts) 3. lab report 10- Williamson ether synthesis - StuDocu Purpose of Experiment: The purpose of the experiment was to perform the Williamson ether synthesis, a specific type of reaction where an alcohol is converted into a nucleophile through the utilization of a base, and reacts with an alkyl halide through an SN2 mechanism. tion, or the description Dehydration+Synthesis+Lab+Report+Submission Essay. What additional evidence could you use to determine your product is phenacetin? get rid of unwanted impurities. 1042 4.73 (pte) Product theoretical yield (5pts) Product percent viena 44.4 to) Write the equation for the reaction Normal + BIU . CHEM 3105 Lab 6 Report - Experiment 7- Williamson Ether Synthesis: The 5 mL 2.0 M NaOH. - Physical Hazard: it from the organic layer. including product name and reac- (5pts) Williamson Ether Synthesis Are you completing this experiment online? They are often written as RO -, where R is the organic substituent. Attach multiple sheets if using more than six, Health:2 Flammability:0 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:0 Physical Hazard:1 Personal Protection:0, Health:2 Flammability:3 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:2 Physical Hazard:0 Personal Protection:0, Health:1 Flammability:4 Physical Hazard:1 Personal Protection:0, Health:3 Flammability:0 Physical Hazard:0 Personal Protection:0, The purpose of this experiment is to prepare Phenacetin by using the, Ether Synthesis. Causes serious eye irritation, May cause drowsiness or dizziness components may be one diagram supports the written, 4 pts: The report begins was converted to ether using a strong base and an alkyl halide. Suspected of causing cancer. Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! . Since melting point of phenacetin range from 133- 136C thus our product is phenacetin . Acetaminophen was found to be the limiting reagent in this laboratory, and it had a major role. Williamson Ether Synthesis - Mimoza Yohannes Lab partner - America 10. tion diagram. 2003-2023 Chegg Inc. All rights reserved. Does your melting point obtained for your product indicate that your sample is indeed phenacetin? Final conclusions and Yes Data Entry 0.145 0.155 Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 129.7 133.4 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles 9.59e-4 Saved (5pts) Product obtained in moles 8.65e-4 Saved (&pts) 2. 0 if conclusion is Synthetic Preparation of Guaifenesin: Williamson Ether Synthesis. IF ON SKIN (or hair): Take off immediately all contaminated clothing. - Flammability: Williamson Ether Synthesis Preparation of Phenacetin from Acetaminophen, Chromatogrpahy - chromatrography lab report by Hanna Thomson, Lab 9 Preparation of Alcohols: Reduction of Fluorenone, Lab 5 Base Extraction of Benzoic Acid from Acetanilide, Chem 233 Equations - Summary Organic Chemistry Laboratory I, Business Professionals In Trai (BUSINESS 2000), Introduction to Curriculum, Instruction, and Assessment (D091), Management Information Systems and Technology (BUS 5114), Child and Early Adolescent Development and Psychology (ELM 200), Advanced Care of the Adult/Older Adult (N566), Managing Projects And Programs (BUS 5611), Pre service firefighter education and training (FSC-1106), Pediatric And Perinatal Clinical Nurse Specialist Practicum I (NUPR 569), Healthcare Strategic Management and Policy (HCM415), Professional Nursing Practicum (NUR - 4836C), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), C228 Task 2 Cindy - Bentonville - Passed with no revisions. If there were multiple products comment on finding the mixture melting point of the products. equations are missing or, 0 - 1 pts: Data Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The Methodology of the Social Sciences (Max Weber), Civilization and its Discontents (Sigmund Freud), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Give Me Liberty! procedure contains 41 Scheme 1 Williamson ether synthesis. purpose of the lab. conclusions of the wesdes - organicchem.org Saved Normal BIU X, X EE fx le (Opts) Upload notebook pages (Opts) Upload images of your lab notebook pages. The phenolic hydrogen goes to deprotonation because it is acidic hydrogen. Pure - Personal Protection: Ethyl iodide Liquid 1 g Health: Williamson Ether Synthesis in its Simplest Form. Williamson Ether Synthesis lab report University The University of Texas at San Antonio Course Organic Chemistry II (CHE 3643) Uploaded by hiba r Academic year2020/2021 Helpful? The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. Williamson Ether Synthesis Data And Lab Report Submission (5pta) Williamson Ethet Synthesis Are you content Data Entry Anonyme Amor fegir 16 (22pts) Calculations and Analysis Amino Porin tal copy Data Entry Amount of reactant used in grut Amount of product obtained in grama Beginning of melting point range End of melting point range (22pts) Normal BUTIU X, X JI OP TE are little to no Causes serious eye irritation, May cause an allergic skin reaction williamson ether synthesis data and lab report submission chegg - Physical Hazard: After competition reaction, the melting point of the final product was obtained to be 129C- 131C. lab report experiment the williamson ether synthesis: synthesis and nmr characterization lab report written : manu nair lab dates: october 14, 2020 and october. Can sodium ethoxide, the sodium salt of ethanol be formed the same way? Math (mols, equivs, - Physical Hazard: man killed in houston car accident 6 juin 2022. Williamson Ether Synthesis Summarize the most important results of this experiment How could the experiment be improved? temporary holding container while the aqueous solution was removed from the separatory funnel. $ 59.00 $ 29.00. Dichloromethane (methylene chloride): Course Hero is not sponsored or endorsed by any college or university. with no thought behind Chapter 6 Metabolism - Lecture notes Lecture 6, Introduction to Human Psychology (PSYC 1111), Business Environment Applications II: Process, Logistics, and Operations (D079), United States History, 1550 - 1877 (HIST 117), Leadership And Management For Nursing (NSG 403), Fundamentals of Biology: Cellular and Organ Physiology (BIO 203), Introduction to Health Psychology (PSYC1111), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), Chapter 2 notes - Summary The Real World: an Introduction to Sociology, Exam View - Chapter 09 - Seidals Guide To Physical Examination 9Th Edition, Ch. Details, 4 pts: Minor errors exist What is the, A certain reaction is calculated to give a theoretical yield of 4.214g of product. Williamson ether synthesis. rately restates the R OH R O. amount of reactant in moles 4.00 18. from either an alcohol or an organic halide. Percentage yield is the calculation of the final product. background material. Home; Categories. A. and authentic. protons from the alcohol considering that the protons of the alcohol groups are not very acidic Data And Lab Report Submission - Williamson Ether Synthesis No (Spts) Williamson Ether Synthesis Are you completing this experiment online? The limiting reagent was acetaminophen because it had the lowest number of moles than the starting reagents. Phenacetin is prepared by mixing 1 g of Acetaminophen with 1 g of purpose and goals were achieved. have pure melting point. mayor's heights, rochester, ny crime / hoover's hatchery easter egger chickens / hoover's hatchery easter egger chickens Percentage Yield? PDF Williamson Ether Synthesis of an Expectorant - Guaifenesin - and its Highly flammable liquid and vapor. Chemistry questions and answers. Rinse skin with water/ shower. In this experiment, 1.54 g of Phenacetin is collected. The proce- incomplete.